Re: [問題] 關於毒奶粉
引用相關paper 的內容,大家自行參考,底下相關的參考文獻我也附上去了,請各位詳閱
(由於是版權物,我找了好久才找到人抓來給我,所以就不能直接分享,台大沒有買此期刊
)
另外~~我也開了關於食品安全資訊板面連署,請大家多多支持,為了你我健康,食品安
全多盡一分心力。
請大家到: LifeNewboard 幫我連署新板
這個是為了你我的知的資訊一起連署,也歡迎一同加入。
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英文名稱: foodsafe
中文名稱: 食品安全資訊交流區
看板類別: 生活/美食/資訊
板主名單: kissinwang
申請原因:
從早期的千面人蠻牛事件,到現今的毒奶粉以及黃麴毒素相關食品
的影響,消費者對於目前的食品安全亮起了大大紅燈,而政府推廣
食品安全履歷到基因改造食品等等,民眾可以得到相關的資訊除了
官網(衛生署相關)之外,可以交流討論的地方卻沒有,而PTT有著營
廣大的群眾,希望藉由這個板的成立讓大家更容易了解食品安全資
連署結束時間: (1223493360)10/09/2008 03:16:00 Thu
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1.kissinwang 食品安全資訊需要大家的支持。 來源:140.112.98.14
Melamine (1,3,5-triazine-2,4,6-triamine) is a nitrogen-based industrial
chemical. It has been used in the manufacture of durable plastics such as
table ware and cups. This use has led to a concern that melamine could
migrate into food coming in contact with these plastics (1–4). Melamine can
also be formed from the degradation of cyromazine, a larvacide used to
prevent flies from hatching (5). High and continuous dietary exposure to
melamine causes formation of bladder stones and increases incidence of
urinary bladder tumors in male rats (6, 7). To date, no studies using human
subjects have been reported.
On March 15, 2007, a pet food manufacturer (Menu Foods, Ontario, Canada)
alerted the U.S. Food and Drug Administration (FDA) to 14 animal deaths in the
United States that appeared to be linked to pet food. In the following months,
consumers and veterinarians reported more illnesses and deaths potentially
associated with pet food. The FDA found melamine and melamine-related
compounds such as cyanuric acid, ammeline, and ammelide in the pet food
samples.
Further investigation showed that some wheat gluten and rice protein imported
from China as pet food ingredients were contaminated with melamine. Melamine
and melamine-related compounds are not approved for use as an ingredient in
pet food (8).
Melamine in matrixes such as Chinese cabbage (9), soil (10), poultry meat(11),
beverages (12), and catfish (13) has been determined by gas chromatography
(GC), GC/mass spectrometry (GC/MS), high-performance liquid chromatography
(HPLC) with UV detection, and LC tandem mass spectrometry (LC/MS/MS).
Determination of melamine in pet food samples has been conducted by the FDA
using an HPLC-UV procedure for quantitation and GC/MS for confirmation (14,15)
However, currently there is no official method for melamine determination in
pet food. This paper describes a new enzyme immunoassay (EIA) procedure and
an HPLC-diode array detection (DAD) method that can be used to determine
melamine in pet food.
EIA is a good screening procedure because of its simplicity and low cost per
analysis, and HPLC-DAD can be used for confirmation and quantification.
Ultra-performance LC coupled with MS/MS (UPLC-MS/MS) was also tested for
correlation with EIA and HPLC-DAD for melamine analysisof pet food.
References
(1) Bradley, E.L., Boughtflower, V., Smith, T. L., Speck, D.R., & Castle, L.
(2005) Food Addit. Contam. 22, 597–606
(2) Kawai, S., Nagano, H., & Maji, T. (1989) J. Chromatogr.
477, 467–470
(3) Lund, K.H., & Petersen, J.H. (2006) Food Addit. Contam. 23,
948–955
(4) Martin, R.E., Hizo, C.B., Ong, A.M., Alba, O.M., & Ishiwata, H. (1992) J.
Food Prot. 55, 632–635
(5) Cabras, P., Meloni, M., & Spanedda, L. (1990) J.
Chromatogr. 505, 413–416
(6) OECD Screening Information DataSet (SIDS) Analysis:
Melamine (June 2002) United Nations Environment Program, http://www.inchem.org/pages/sids.html
(7) International Agency for Research on Cancer (1999) Vol. 73, IARC, Lyon, France
(8) http://www.fda.gov/cvm/MenuFoodRecallFAQ.htm
(9) Bardalaye, P.C., Wheeler, W.B., & Meister, C.W. (1987) J.
Assoc. Off. Anal. Chem. 70, 455–457
(10) Yokley, R.A., Mayer, L.C., Rezaaiyan, R., Manuli, M.E., & Cheung, M.W.
(2000) J. Agric. Food Chem. 48, 3352–3358
(11) Chou, S., Hwang, D., & Lee, H. (2003) J. Food Drug Anal.
11, 290–295
(12) Ishiwata, H., Inoue, T., Yamazaki, T., & Yoshihira, K. (1987) J. Assoc.
Off. Anal. Chem. 70, 457–460
(13) Andersen, W.C., Turnipseed, S.B., Karbiwnyk, C.M., & Madson, M.R. (2007) U.S. FDA Laboratory Information Bulletin 23, No. 4396
(14) Updated FCC Developmental Melamine Quantitation
(HPLC-UV) (April 2, 2007) http://www.fda.gov/cvm/melamine04022007.htm
(15) GC/MS Screen for the Presence of Melamine, Ammeline, Ammelide and Cyanuric Acid (Version 2.1), http://www.fda.gov/cvm/GCMSMelamine.htm
引用內容:
Kim, B., Perkins, L. B., Bushway, R. J., Nesbit, S., Fan, T., Sheridain, R., & Greene, V. (2008). Determination of melamine in pet food by enzyme immunoassay, high-performance liquid chromatography with diode array detection, and ultra-performance liquid chromatography with tandem mass spectrometry. Journal of Aoac International, 91(2), 408-413.
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